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10.6 Corrosion of Hastelloy N and Other Alloys in Steam77

10.7 Intergranular Cracking of Alloys Exposed to Tellurium79

10.8 Chemistry of Salt-Metal-Tellurium System79

10.9 Auger Observations Relative to Intergranular Cracking80

10.9.1 Fracture Surface Analysis81

10.9.2 High Temperature Surface Studies81

10.10 In-Reactor Fueled Experiments81

10.10.1 Design82

10.10.2 Calculated Operation and Test Conditions82

10.10.3 Preliminary Operating Data84

11. FUEL PROCESSING MATERIALS DEVELOPMENT86

11.1 Static Capsule Tests of Graphite with Bismuth and Bismuth-Lithium Solutions86

11.2 Thermal Convection Loop Tests of Molybdenum, Tantalum, and Graphite in

Bismuth-Lithium Solution89

12. GRAPHITE STUDIES92

12.1 Property Changes in Near-Isotropic Grades of Graphite Irradiated at 715°C to Fluences

as High as 4.2x1022 neutrons/cm292

12.1.1 Materials92

12.1.2 Testing94

12.1.3 Property Changes as Functions of Fluence95

12.1.4 Conclusions95

PART 4. FUEL PROCESSING FOR MOLTEN-SALT REACTORS

13. PROCESSING CHEMISTRY100

13.1 Chemistry of Fluorination and Fuel Reconstitution100

13.2 Equilibria in Fused Salt-Liquid Alloy Systems101

14. ENGINEERING DEVELOPMENT OF PROCESSING OPERATIONS102

14.1 Examination of Equipment from Metal Transfer Experiment MTE-3102

14.2 Installation of Metal Transfer Experiment MTE-3B112

14.3 Design of the Metal Transfer Process Facility114

14.4 Salt-Metal Contactor Development: Experiments with a Mechanically Agitated

Nondispersing Contactor in the Salt-Bismuth Flow-through Facility114

14.5 Salt-Metal Contactor Development: Experiments with a Mechanically Agitated

Nondispersing Contactor Using Water and Mercury119

14.5.1 Theory119

14.5.2 Experimental Apparatus121

14.5.3 Results and Conclusions121

14.6 Continuous Fluorinator Development: Autoresistance Heating Test AHT-3122

14.6.1 Experimental Equipment and Procedure122

14.6.2 Experimental Results124

14.6.3 Distribution of Current Densities in the Autoresistance Heating Equipment124

14.7 Fuel Reconstitution Development: Design of a Fuel Reconstitution Engineering Experiment127

14.8 Performance of Open Bubble Columns129

14.8.1 Axial Dispersion in Open Bubble Columns130

14.8.2 Mass Transfer Rates in Open Bubble Columns130

14.9 Conceptual Design of an MSBR Processing Engineering Laboratory132

PART5. SALT PRODUCTION

15. PRODUCTION OF FLUORIDE-SALT MIXTURES FOR RESEARCH

AND DEVELOPMENT PROGRAM134

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