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MOLTEN-SALT REACTOR PROGRAM - page 53 / 122

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Characterization of Hastelloy N for Service at 932°C125

6.8 Thermal Convection Loops130

7. CHEMISTRY134

7.1 Chemistry of the MSRE134

Behavior of Fuel and Coolant Salt134

7.2 Physical Chemistry of Fluoride Melts139

Viscosity and Density of Molten Beryllium Fluoride139

Transpiration Studies in Support of the Vacuum Distillation Process140

Estimated Thermophysical Properties of MSBR Coolant Salt141

7.3 Separation in Molten Fluorides142

Extraction of Rare Earths from Molten Fluorides into Molten Metals142

Removal of Rare Earths from Molten Fluorides by Simultaneous Precipitation with UF3145

Removal of Protactinium from Molten Fluorides by Oxide Precipitation147

Extraction of Protactinium from Molten Fluorides into Molten Metals148

Protactinium Studies in the High-Alpha Molten-Salt Laboratory156

7.4 Radiation Chemistry158

Xenon Diffusion and Possible Formation of Cesium Carbide in an MSBR158

Fission Product Behavior in the MSRE165

7.5 Development and Evaluation of Analytical Methods for Molten-Salt Reactors191

Determination of Oxide in Radioactive MSRE Samples191

Spectrophotometric Studies of Molten-Salt Reactor Fuels193

Voltammetric and Chronopotentiometric Studies of Uranium in Molten LiF-BeF2-ZrF4195

In-Line Test Facility196

Analysis of Helium Blanker Gas196

7.6 Development and Evaluation of Equipment and Procedures

for Analyzing Radioactive MSEE Salt Samples199

Sample Analyses200

Quality-Control Program200

Part 3. MOLTEN-SALT BREEDER REACTOR STUDIES

8. MOLTEN-SALT BREEDER REACTOR DESIGN STUDIES207

8.1 Design Changes in MSBR Plant207

8.2 Modular-Type Plant212

8.3 Steam Cycle with Alternative Feedwater Temperature217

8.4 Additional Design Concepts223

9. MOLTEN-SALT REACTOR PROCESSING STUDIES227

9.1 Semicontinuous Distillation228

9.2 Continuous Fluorination of a Molten Salt232

9.3 Alternative Chemical Processing Methods for an MSBR233

Reduction Precipitation235

Li-Bi Alloy Extraction237

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