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U(IV)/U(III) Couple in Molten LiF-BeF2 -ZrF4201

14.4 Emf Measurements in Molten Fluorides202

14.5 Development of a Molten-Salt Spectrophotometric Facility for Hot-Cell Use202

14.6 Absorption Spectra of 3d Transition-Metal Ions in Molten LiF-BeF2204

14.7 Effect of Reductants on Metal-Fluoride-Salt Wetting Behavior205

14.8 Determination of Contaminants in the Blanket Gas of NaBF4 Tests205

14.9 Determination of Bismuth in MSRP Salts208

14.9.1 Polarography208

14.9.2 Spectrophotometry208

14.9.3 Emission Spectrography208

14.9.4 Polarographic Shipping208

14.9.5 Isotopic Exchange208

PART 4. MOLTEN-SALT IRRADIATION EXPERIMENTS

15. MOLTEN-SALT CONVECTION LOOP IN ORR210

15.1 Studies of Surface Wetting of Graphite by Molten Salt210

PART 5. MATERIALS DEVELOPMENT

16. MSRE SURVEILLANCE PROGRAM211

16.1 Examination of Particles Removed from Pump Bowl with Magnets211

16.1.1 Observations on Particles from Magnet FP-15-53212

16.1.2 Observations on Particles from Magnet FP-16-2213

17. GRAPHITE STUDIES214

17.1 Fundamental Studies of Radiation Damage Mechanisms in Graphite214

17.2 Graphitization Chemistry and Binder System Development215

17.3 Hot Pressing of Graphite Pellets Using Various Binders216

17.4 Procurement and Physical Property Measurements on New Grades of Graphite217

17.5 Physical Properties of Graphites219

17.6 X-Ray Studies219

17.7 Electron Microscopy of Graphite221

17.8 Gas Impregnation of Graphite with Carbon221

17.9 Graphite Irradiation in HFIR224

17.10 Calculation of Lifetime and Induced Stresses in MSBR Cores229

18. HASTELLOY N232

18.1 Influence of Titanium and Carbon on the Mechanical Properties of Nickel-Base Alloys232

18.2 Aging of Modified Hastelloy N233

18.3 Influence of Irradiation Temperature on the Creep-Rupture Properties of Hastelloy N235

18.4 Electron Microscopy Studies240

18.5 Measurement of Residual Stresses in Hastelloy N Welds242

18.6 Corrosion Studies243

18.6.1 Fuel Salts243

18.6.2 Fertile-Fissile Salts243

18.6.3 Blanket Salts245

18.6.4 Coolant Salts246

18.6.5 Comparison of the Kinetic Behavior of Nickel- and Iron-Based

Alloys in Molten Fluoride Salts248

18.7 Forced Convection Loop253

18.8 Oxidation of Hastelloy N254

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