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MOLTEN-SALT REACTOR PROGRAM - page 93 / 122

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15.8.1 Results of Thermal Convection Loop Tests166

15.8.2 Fertile-Fissile Salt168

15.8.3 Blanket Salt168

15.8.4 Coolant Salt168

15.8.5 Summary171

15.9 Forced-Convection Loop, MSR-FCL-1173

15.9.1 Operations173

15.9.2 Cold Finger Corrosion Product Trap174

15.9.3 Metallurgical Analysis175

15.9.4 Forced-Convection Loop MSR-FCL-2176

15.10 Corrosion of Hastelloy N in Steam178

15.11 Evaluation of Duplex Tubing for Use in Steam Generators181

16. SUPPORT FOR CHEMICAL PROCESSING184

16.1 Construction of a Molybdenum Reductive Extraction Test Stand184

16.2 Fabrication Development of Molybdenum Components184

16.3 Welding of Molybdenum185

16.4 Development of Bismuth-Resistant Filler Metals for Brazing Molybdenum189

16.5 Compatibility of Structural Materials with Bismuth189

16.6 Chemically Vapor Deposited Coatings195

16.6.1 Tungsten Coatings195

16.6.2 Molybdenum Coatings197

16.7 Molybdenum Deposition from MoF6197

17. FLOWSHEET ANALYSIS199

17.1 Protactinium Isolation Using Fluorination-Reductive Extraction200

17.2 Rare-Earth Removal Using the Metal Transfer Process201

17.3 Removal of Uranium from Fuel Salt by Oxide Precipitation202

18. MEASUREMENT OF DISTRIBUTION COEFFICIENTS IN MOLTEN-SALT-METAL SYSTEMS204

18.1 Metal Transfer Process Studies204

18.2 Solubility of Neodymium in Li-Bi-Th Solutions207

18.3 Solubility of LaOCl in Molten LiCl208

18.4 Oxide Precipitation Studies208

PART 5. MOLTEN-SALT PROCESSING AND PREPARATION

19. ENGINEERING DEVELOPMENT OF PROCESS OPERATIONS211

19.1 Reductive Extraction Engineering Studies211

19.2 Design of a Processing Materials Test Stand and the Molybdenum Reductive

Extraction Equipment212

19.3 Contactor Development: Pressure Drop, Holdup, and Flooding in Packed Columns213

19.4 Contactor Development: Axial Mixing in Packed Columns215

19.5 Axial Mixing in Open Bubble Columns216

19.6 Demonstration of the Metal Transfer Process for Rare-Earth Removal217

19.7 Development of a Frozen-Wall Fluorinator219

19.8 Electrolytic Cell Development220

20. CONTINUOUS SALT PURIFICATION SYSTEM224

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